Brandeis Search
Time Request Form for Brandeis Researcher 1. Investigator Information - provide the following information for each investigator [required] Name of primary investigator: 2. Funding for this project [required] Grant Title: Agency: Agency Grant Number: 3. Billing information[required]- if multiple grants should be charged please indicate percentages Charge Line: 4. Spectrometer operator Name of primary operator: Email: Phone: 5. Which spectrometer are you requesting time for? - please check appropriate box [required] Avance 800 Please select a probe 5mm TCI CryoProbe with z-grad 5mm QXI 1H/31P {15N/13C} z-grad 6. Time requested [required] Number of days requested: Dates requested: Earliest date sample would be ready: 7. Other comments (dates not available, etc.) 8. Sample description [required] Sample identity Solvent Concentration Temperature Special handling/storage required 9. Experiment description [required] A. Provide a complete description of your experiments. Please include a brief justification for the use of this facility, as well as the field strength and the time requested. B. Indicate the name of the standard Bruker pulse program(s) you plan to use. (Download of list of standard Bruker sequences) C. If you are not using one of the standard Bruker pulse sequences, please give a detailed description of your NMR experiments, including literature references (if previously published), pulse scheme (if unpublished or modified experiment), solvent suppression scheme, use of pulsed field gradients, deuterium decoupling, etc. You must either write the pulse program yourself or make prior arrangements with Prof. Sue Pochapsky. 10. Do you request training? (select appropriate button) [required] yes no 11. What assistance is requested? [required] none Or assistance with (select all that apply) Sample set-up None Changing sample Tuning probe Locking Shimming Acquisition None Bruker acquisition software Choosing pulse sequence Parameter setup Pulse width calibrations Writing/implementing pulse program Using pulsed field gradients Processing None TOPSPIN software Other
